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<span style="font-family:宋体;font-size:12pt;">游离基反åº?/span><span style="font-size:12pt;"></span> </p> <p class="MsoNormal"> <span style="font-size:12pt;"><span>    </span></span><span style="font-family:宋体;font-size:12pt;">铄¡š„引发</span><span style="font-size:12pt;"></span> </p> <p class="MsoNormal"> <span style="font-size:12pt;"><span>    </span></span><span style="font-family:宋体;font-size:12pt;">˜qžçš„增长</span><span style="font-size:12pt;"></span> </p> <p class="MsoNormal"> <span style="font-size:12pt;"><span>    </span></span><span style="font-family:宋体;font-size:12pt;">铄¡š„¾lˆæ­¢</span><span style="font-size:12pt;"></span> </p> <p class="MsoNormal"> <span style="font-size:12pt;">2</span><span style="font-family:宋体;font-size:12pt;">、工è‰ø™¿‡½E?/span><span style="font-size:12pt;"></span> </p> <p class="MsoNormal"> <span style="font-family:宋体;font-size:12pt;">配料æ¯?/span><span style="font-size:12pt;"></span> </p> <p class="MsoNormal"> <span style="font-size:12pt;"><span>    </span></span><span style="font-family:宋体;font-size:12pt;"><a href="/dxjyb/" target="_blank">对硝åŸÞZ¹™è‹?/a></span><span style="font-size:12pt;">:</span><span style="font-family:宋体;font-size:12pt;">½Iºæ°”</span><span style="font-size:12pt;">:</span><span style="font-family:宋体;font-size:12pt;">¼‹¬è„‚é…”R’´</span><span style="font-size:12pt;">:</span><span style="font-family:宋体;font-size:12pt;">醋酸é”?/span><span style="font-size:12pt;">=1:</span><span style="font-family:宋体;font-size:12pt;">适量</span><span style="font-size:12pt;">:5.33</span><span style="font-family:宋体;font-size:12pt;">×</span><span style="font-size:12pt;">10-5: 5.33</span><span style="font-family:宋体;font-size:12pt;">×</span><span style="font-size:12pt;">10-5</span> </p> <p class="MsoNormal"> <span style="font-family:宋体;font-size:12pt;">加料</span><span style="font-size:12pt;"></span> </p> <p class="MsoNormal"> <span style="font-family:宋体;font-size:12pt;">通空气、搅æ‹?/span><span style="font-size:12pt;"></span> </p> <p class="MsoNormal"> <span style="font-family:宋体;font-size:12pt;">定期化验反应液中的含酮量与含酔R‡</span><span style="font-size:12pt;"></span> </p> <p class="MsoNormal"> <span style="font-family:宋体;font-size:12pt;">反应¾lˆç‚¹åQšå½“含酮量由高峰开始下é™?/span><span style="font-size:12pt;"></span> </p> <p class="MsoNormal"> <span style="font-family:宋体;font-size:12pt;">½Eå†·ã€å¸æ–?/span><span style="font-size:12pt;"></span> </p> <p class="MsoNormal"> <span style="font-size:12pt;">80-90</span><span style="font-family:宋体;font-size:12pt;">℃下¾~“缓加入¼„³é…¸é’ é¥±å’Œæ°´æº¶æ¶²è°ƒè‡³</span><span style="font-size:12pt;">pH7.8-8</span> </p> <p class="MsoNormal"> <span style="font-family:宋体;font-size:12pt;">冷却臛_®¤æ¸©ï¼Œå†·å†»è‡?/span><span style="font-size:12pt;">-3 </span><span style="font-family:宋体;font-size:12pt;">℃结晶过æ»?/span><span style="font-size:12pt;"></span> </p> <p class="MsoNormal"> <span style="font-family:宋体;font-size:12pt;">溶解ã€?/span><span style="font-size:12pt;">15%</span><span style="font-family:宋体;font-size:12pt;">¼„³é…¸é’ è°ƒ</span><span style="font-size:12pt;">pH7-7.5,</span><span style="font-family:宋体;font-size:12pt;">冯‚‡³</span><span style="font-size:12pt;">5</span><span style="font-family:宋体;font-size:12pt;">℃,˜q‡æ×o</span><span style="font-size:12pt;"></span> </p> <p class="MsoNormal"> <span style="font-family:宋体;font-size:12pt;">‹z—æá”、干ç‡?/span><span style="font-size:12pt;"></span> </p> <p class="MsoNormal"> <span style="font-family:宋体;font-size:12pt;">å¾?a href="/dxjbyd/" target="_blank">对硝åŸø™‹¯ä¹™é…®</a></span><span style="font-size:12pt;"></span> </p> <p class="MsoNormal"> <span style="font-size:12pt;"><span>    </span></span><span style="font-family:宋体;font-size:12pt;">熔点</span><span style="font-size:12pt;">78-80</span><span style="font-family:宋体;font-size:12pt;">℃、含é‡?/span><span style="font-size:12pt;">96%</span><span style="font-family:宋体;font-size:12pt;">以上、收çŽ?/span><span style="font-size:12pt;">57-58.7%</span> </p> <p class="MsoNormal"> <span style="font-family:宋体;font-size:12pt;">滤液酸化回收对硝åŸø™‹¯ç”²é…¸</span><span style="font-size:12pt;"></span> </p> <p class="MsoNormal"> <span style="font-size:12pt;">3</span><span style="font-family:宋体;font-size:12pt;">、反应条件及影响因素</span><span style="font-size:12pt;"></span> </p> <p class="MsoNormal"> <span style="font-family:宋体;font-size:12pt;">åQ?/span><span style="font-size:12pt;">1</span><span style="font-family:宋体;font-size:12pt;">åQ‰å‚¬åŒ–剂的作ç”?/span><span style="font-size:12pt;"></span> </p> <p class="MsoNormal"> <span style="font-size:12pt;"><span>    </span></span><span style="font-family:宋体;font-size:12pt;">¼‹¬è„‚é…”R’´å…ähœ‰å‚¬åŒ–性能好,选择性高åQŒäñ”物对¼‹åŸºè‹¯ä¹™é…®å«é‡é«˜åQŒå‰¯äº§ç‰©å«é‡ä½?/span><span style="font-size:12pt;"></span> </p> <p class="MsoNormal"> <span style="font-size:12pt;"><span>    </span></span><span style="font-family:宋体;font-size:12pt;">催化剂用量少、反应温度低、反应速度快、周期短、反应åã^½EÏx˜“控制åQŒäñ”区的质量提高</span><span style="font-size:12pt;"></span> </p> <p class="MsoNormal"> <span style="font-family:宋体;font-size:12pt;">åQ?/span><span style="font-size:12pt;">2</span><span style="font-family:宋体;font-size:12pt;">åQ‰ååº”温åº?/span><span style="font-size:12pt;"></span> </p> <p class="MsoNormal"> <span style="font-size:12pt;"><span>    </span></span><span style="font-family:宋体;font-size:12pt;">反应¾l´æŒåœ¨æ—¢ä¸è¿‡åˆ†æ¿€çƒˆåˆå‡åŒ€å‡ºæ°´çš„程åº?/span><span style="font-size:12pt;"></span> </p> <p class="MsoNormal"> <span style="font-family:宋体;font-size:12pt;">åQ?/span><span style="font-size:12pt;">3</span><span style="font-family:宋体;font-size:12pt;">åQ‰ååº”压åŠ?/span><span style="font-size:12pt;"></span> </p> <p class="MsoNormal"> <span style="font-size:12pt;"><span>    </span></span><span style="font-family:宋体;font-size:12pt;">反应分子数减ž®‘的反应åQŒåŠ åŽ‹å¯¹ååº”有利</span><span style="font-size:12pt;"></span> </p> <p class="MsoNormal"> <span style="font-size:12pt;">0.5MPa</span><span style="font-family:宋体;font-size:12pt;">。大äº?/span><span style="font-size:12pt;">0.5MPa</span><span style="font-family:宋体;font-size:12pt;">å¯ÒŽé«˜äñ”物含量不显著</span><span style="font-size:12pt;"></span> </p> <p class="MsoNormal"> <span style="font-family:宋体;font-size:12pt;">åQ?/span><span style="font-size:12pt;">4</span><span style="font-family:宋体;font-size:12pt;">åQ‰æŠ‘制物</span><span style="font-size:12pt;"></span> </p> <p class="MsoNormal"> <span style="font-size:12pt;"><span>    </span></span><span style="font-family:宋体;font-size:12pt;">苯胺、酚¾c…R€é“ç›?/span><span style="font-size:12pt;"></span> </p> <p class="MsoNormal"> <span style="font-family:宋体;font-size:12pt;">注意事项</span><span style="font-size:12pt;"></span> </p> <p class="MsoNormal"> <span style="font-size:12pt;"><span>    </span></span><span style="font-family:宋体;font-size:12pt;">¼‹¬è„‚酸质轻,为防止投料飞扬损失,预先ž®†å…¶ä¸Žç­‰é‡çš„对硝åŸÞZ¹™è‹¯æ‹Œå’Œï¼Œç„¶åŽåŠ å…¥ååº”å¡?/span><span style="font-size:12pt;"></span> </p></p> <p><div>上一æ?<a 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